Crystal structure of (2S,4S,7S)-7,7-dichloro-4-(1-chloro-1-methylethyl)- 1-(2,2,2-trichloroethyl)bicyclo[4.1.0]heptane, C12H16Cl6

Boualy, Brahim; Firdoussi, Larbi El; Ali, Mustapha Ait; Karim, Abdallah; Spannenberg, Anke

doi:10.1524/ncrs.2009.0278

Zeitschrift Für Kristallographie - New Crystal Structures

2009

DOI: 10.1524/ncrs.2009.0278

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Crystal structure of (2S,4S,7S)-7,7-dichloro-4-(1-chloro-1-methylethyl)- 1-(2,2,2-trichloroethyl)bicyclo[4.1.0]heptane, C₁₂H₁₆Cl₆

Brahim Boualy¹,

Larbi El Firdoussi²,

Mustapha Ait Ali³

et al.

Abstract: Abstract

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2012

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(R)-2-Methyl-5-[(R)-2,4,4,4-tetrachlorobutan-2-yl]cyclohex-2-enone

Boualy¹,

Harrad²,

Firdoussi³

et al. 2012

Acta Cryst E

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The title compound, C11H14Cl4O, was efficiently synthesized by atom-transfer radical addition between (R)-carvone and tetrachloromethane. In the molecule, both chiral centres are of the absolute configurationR. The cyclohex-2-enone ring has an envelope conformation with the chiral C atom displaced by 0.633 (2) Å from the mean plane through the other five C atoms [maximum deviation = 0.036 (2) Å]. In the crystal, molecules are linkedviaC—H...O interactions, leading to the formation of helical chains propagating along [100].

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(R)-2-Methyl-5-[(R)-2,4,4,4-tetrachlorobutan-2-yl]cyclohex-2-enone

Boualy¹,

Harrad²,

Firdoussi³

et al. 2012

Acta Cryst E

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Crystal structure of (2S,4S,7S)-7,7-dichloro-4-(1-chloro-1-methylethyl)- 1-(2,2,2-trichloroethyl)bicyclo[4.1.0]heptane, C₁₂H₁₆Cl₆

Abstract: Abstract

Cited by 1 publication

References 3 publications

(R)-2-Methyl-5-[(R)-2,4,4,4-tetrachlorobutan-2-yl]cyclohex-2-enone

(R)-2-Methyl-5-[(R)-2,4,4,4-tetrachlorobutan-2-yl]cyclohex-2-enone

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