Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ2
 O,O′) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4
 N,N′,N′′,N′′′)]nickel(II) perchlorate, C29H50Cl2N4NiO8

Ou, Guang‐Chuan; Jia, Guo-Kai; Tan, Ying-Zhi

doi:10.1515/ncrs-2019-0236

Zeitschrift Für Kristallographie - New Crystal Structures

2019

DOI: 10.1515/ncrs-2019-0236

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Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ² O,O′) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴ N,N′,N′′,N′′′)]nickel(II) perchlorate, C₂₉H₅₀Cl₂N₄NiO₈

Guang‐Chuan Ou

Guo-Kai Jia

Ying-Zhi Tan

Abstract: C29H50Cl2N4NiO8, orthorhombic, Pbca (no. 61), a = 20.601(3) Å, b = 13.5059(16) Å, c = 25.015(3) Å, Z = 8, V = 6960.3(15) Å3, Rgt(F) = 0.0495, wRref(F2) = 0.1652, T = 296(2) K.

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Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ² O,O′) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴ N,N′,N′′,N′′′)]nickel(II) perchlorate, C₂₉H₅₀Cl₂N₄NiO₈

Abstract: C29H50Cl2N4NiO8, orthorhombic, Pbca (no. 61), a = 20.601(3) Å, b = 13.5059(16) Å, c = 25.015(3) Å, Z = 8, V = 6960.3(15) Å3, Rgt(F) = 0.0495, wRref(F2) = 0.1652, T = 296(2) K.

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References 5 publications

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Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ2 O,O′) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4 N,N′,N′′,N′′′)]nickel(II) perchlorate, C29H50Cl2N4NiO8

Abstract: C29H50Cl2N4NiO8, orthorhombic, Pbca (no. 61), a = 20.601(3) Å, b = 13.5059(16) Å, c = 25.015(3) Å, Z = 8, V = 6960.3(15) Å3, Rgt(F) = 0.0495, wRref(F2) = 0.1652, T = 296(2) K.

Cited by 0 publications

References 5 publications

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Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ² O,O′) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴ N,N′,N′′,N′′′)]nickel(II) perchlorate, C₂₉H₅₀Cl₂N₄NiO₈