Abstract:Single crystals of destripeptide (B28-B30) insulin (DTRI) in three forms were obtained by hanging-drop vapor diffusion method. Form 1 belongs to P2 1 space group with cell parameters a=4.77 nm b=6.19 nm c=6.12 nm β=110.3 o . Form 2 belongs to P4 1 22 or P4 3 22 space group with cell parameters a= 6.45 nm, c=12.07 nm. Form 3 belongs to P2 1 2 1 2 1 space group with cell parameters a=4.98 nm b=5.16 nm c=10.06 nm. The structure of form 1 crystal was determined by molecular replacement method and refined at 0.23 n… Show more
“…The preparation and crystallization of recombinant DTRI was as described earlier [11,17]. The crystals were grown by the hanging drop vapor di¡usion method.…”
“…The preparation and crystallization of recombinant DTRI was as described earlier [11,17]. The crystals were grown by the hanging drop vapor di¡usion method.…”
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