Abstract:6a-Bromo-I 7@-hydroxy-I 7a-methyl-Paul," W. A. Noyes Chemical Laboratory, University of The crystal and molecular structure of 6a-bromo-l7~-hydroxy-l7a-methyl-4-oxa-5a-androstan-3-one (I) has been determined by three-dimensional X-ray analysis. The crystals of (I) are orthorhombic with a = 12.23, b = 7.30, and c = 20.1 4 8, and the space group is P212121 with Z = 4. The structure has been refined to an R of 0.1 2 on 1500 reflexions collected photographically. The A : B, B : C, and C : D ring junctions are all … Show more
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