2016
DOI: 10.1515/revce-2015-0047
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Crosslinking of starch and its effect on viscosity behaviour

Abstract: AbstractStarch is a widely used component in the food industry. Native starch does not have the desired properties, so it is modified according to the required properties. Out of different methods, crosslinking is one of the widely used ones. There are different crosslinking agents available. The method and mechanism of widely used crosslinking agents like phosphorous oxychloride, adipate and epichlorohydrin are discussed and compared. When starch is crosslinked, its properties… Show more

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Cited by 78 publications
(44 citation statements)
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“…The extent and yield of cross‐linking of starch are often difficult to measure chemically, and hence, physical properties measurement is usually preferred. [ 22,26 ] There are some physical indications like changes in starch swelling and solubility, pasting curves, sedimentation volume, optical clarity, and fluidity, which can be taken as indirect measures of cross‐linking extent. [ 22,23 ] In the current contribution, the existence of a concomitant role of tartaric acid (or tartaric acid derivatives formed in situ) as cross‐linking agents of modified starches was evaluated indirectly in terms of starches solubility in DMSO (a solvent of common use for native and esterified starches), swelling power, resistance to the action of amylase enzymes, and gelatinization behavior.…”
Section: Resultsmentioning
confidence: 99%
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“…The extent and yield of cross‐linking of starch are often difficult to measure chemically, and hence, physical properties measurement is usually preferred. [ 22,26 ] There are some physical indications like changes in starch swelling and solubility, pasting curves, sedimentation volume, optical clarity, and fluidity, which can be taken as indirect measures of cross‐linking extent. [ 22,23 ] In the current contribution, the existence of a concomitant role of tartaric acid (or tartaric acid derivatives formed in situ) as cross‐linking agents of modified starches was evaluated indirectly in terms of starches solubility in DMSO (a solvent of common use for native and esterified starches), swelling power, resistance to the action of amylase enzymes, and gelatinization behavior.…”
Section: Resultsmentioning
confidence: 99%
“…New intra‐ and/or intermolecular bonds introduced during cross‐linking of starch are known to reduce the tendency of starch granules to solubilize and rupture, and to induce resistance to gelatinization provided enough cross‐links bonds are present. [ 22,26,34,56 ] Figure schematizes the starch fractions recovered from the gelatinization assay of MS samples. After centrifugation the supernatants were casted on plastic boxes, showing homogenous film forming capacity.…”
Section: Resultsmentioning
confidence: 99%
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“…The temperature of the reaction is typically 25–50 °C. Depending upon the protocol, the reaction time can vary from 30 min to 24 h. After the reaction is complete, the starch is adjusted to neutral pH, filtered, washed, and dried …”
Section: Classification Of Starch Modificationmentioning
confidence: 99%
“…12 Crosslinking introduces a covalent interconnection via hydrogen bonds in starch granules which provides strong bonds between the molecules and restrict the movement of the polymer chains. [15][16] This decreases the rate of starch retrogradation which consequently increases rigidity and hardness of its gel; in addition to enhancing its solubility in organic solvents. 8,17 Various reagents are used in the crosslinking reaction and these determine the property of the cross-linked product.…”
Section: Introductionmentioning
confidence: 99%