a b s t r a c tMagnetic exchange bias and coercivity of nanogranular NiFe 2 O 4 /NiO thin films, prepared using flowstabilized microplasmas and post-deposition annealing, have been investigated as a function of ferrimagnet/antiferromagnet phase fraction, grain size, and temperature. Exchange bias (EB) and vertical shifts in hysteresis loops observed in the as-deposited and low-T annealed ( r 600°C) films were attributed to exchange coupling between nanocrystalline NiFe 2 O 4 ( $ 8-10 nm) and a structurally-disordered spin glass (SG)-like phase. At higher annealing temperature (850°C), the observed EB was found to arise from exchange coupling between NiFe 2 O 4 and NiO, rather than a SG phase, most likely due to reduction of structurally-disordered interfaces and a substantial increase in NiFe 2 O 4 grain size ( $ 26 nm).