Continuous and Scalable Synthesis of Prussian Blue Analogues with Tunable Structure and Composition in Surfactant‐Free Microreactor for Stable Zinc‐Ion Storage
Mingli Wang,
Jingkang Ma,
Ke Lu
et al.
Abstract:We represent a segmented flow surfactant‐free microfluidic strategy for continuous synthesis of Prussian blue analogues (PBAs) with high dispersity and high crystallization. Representative zinc hexacyanoferrate (ZnHCF) nanocubes were successfully synthesized in a microfluidic reactor within a few minutes via the cooperation method and possessed lower contents of crystal water and Fe(CN)63‐ vacancies than that of synthesis in bulk solution. The nucleation and particle growth process can be precisely controlled … Show more
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