A commercial sample of Cedrelopsis grevei H. Baillon from Madagascar was repeatedly chromatographed and the combined analysis of all the fractions by GC, GC-MS and 13 C-NMR led to the identification of 114 components. The major constituents were (E)-β-caryophyllene (9.3%), α-copaene (7.7%), α-selinene (5.8%), δ-cadinene (4.9%), β-selinene (4.5%), α-humulene (3.3%) and β-bisabolene (2.8%). Analysis of five other commercial samples confirmed the pre-eminence of sesquiterpene hydrocarbons and exhibited a variation in the contents of the main components: ishwarane (1.0-17.4%), (E)-β-caryophyllene (1.3-12.5%), α-copaene (4.9-11.0%), β-elemene (0.2-9.6%) and α-selinene (1.1-9.4%).