Constant rate thermal analysis of a dehydrogenation reaction

Abstract

The kinetic analysis of constant rate thermal analysis (CRTA) curves obtained for MgH2 dehydrogenation under high vacuum reveals that the reaction obeys first-order kinetics.

On the determination of thermal degradation effects and detection techniques for thermoplastic composites obtained by automatic lamination

“…The foundation of this methodology is maintaining the reaction rate at a desired value using a control system that regulates the furnace temperature. It has been demonstrated that the shape of the α-T curves obtained by CRTA allows elucidating the kinetic model followed by the process [41][42][43].…”

Control of experimental conditions in reaction flash-sintering of complex stoichiometry ceramics

“…The electrical properties of the Bi0.93La0.07FeO3 specimen prepared by reaction flash sintering at 100 V cm -1 and 40 mA mm -2 were measured by impedance spectroscopy. This technique has been proved a powerful tool for testing the quality of different kinds of ceramic materials, because it is extremely sensitive to the stoichiometry, the microstructure and the presence of secondary phases and vacancies [38,[54][55][56][57][58][59][60][61][62].…”