Conformational effects in Mn(II)-doped trisethylenediamine zinc(II) and cadmium(II) nitrates

Sastry, Srikanth; Lingam, K. V.; Rao, Minglu

doi:10.1080/00268978300102481

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“…This symmetry change has been assigned on the basis of EPR on nickel(ii)doped [11][12][13] and manganese(ii)-doped [10,14] single crystals * Hexagonal space group P 6 3 22(Z = 2), a = 8.9267(5) Å, c = 11.329(2) Å, V = 781.8 (2) …”

Section: Introductionmentioning

confidence: 99%

Structural Definition of the Low-Temperature Phase Transition of Tris(ethane-1,2-diamine)zinc(II) Dinitrate

Bernhardt¹,

Riley²

2003

Aust. J. Chem.

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The 93 K X-ray crystal structure of tris(ethane-1,2-diamine)zinc(ii) dinitrate is reported. As predicted by the spectroscopic studies of other workers, there is a reversible phase transition of the structure at low temperature. We have determined this temperature to be 143 K. The structure at this temperature and below resembles that of the room temperature structure, except the crystallographic D 3 symmetry of the complex cation (296 K) is lowered to C 2 (below 144 K) by subtle changes in cation-anion hydrogen bonding. No change in the conformation of the cation or its bond lengths and angles was found.

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Section: Introductionmentioning

confidence: 99%

Structural Definition of the Low-Temperature Phase Transition of Tris(ethane-1,2-diamine)zinc(II) Dinitrate

Bernhardt¹,

Riley²

2003

Aust. J. Chem.

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Electron Paramagnetic Resonance of Mn²⁺ in Orthorhombic and Higher Symmetry Crystals

Jain

Lehmann

1990

Physica Status Solidi (b)

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EPR and optical properties of impurity centers in low-symmetry crystals

Viswanath

Radhakrishna

1991

Journal of Physics and Chemistry of Solids

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Conformational effects in Mn(II)-doped trisethylenediamine zinc(II) and cadmium(II) nitrates

Cited by 5 publications

References 19 publications

Structural Definition of the Low-Temperature Phase Transition of Tris(ethane-1,2-diamine)zinc(II) Dinitrate

Structural Definition of the Low-Temperature Phase Transition of Tris(ethane-1,2-diamine)zinc(II) Dinitrate

Electron Paramagnetic Resonance of Mn²⁺ in Orthorhombic and Higher Symmetry Crystals

EPR and optical properties of impurity centers in low-symmetry crystals

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Conformational effects in Mn(II)-doped trisethylenediamine zinc(II) and cadmium(II) nitrates

Cited by 5 publications

References 19 publications

Structural Definition of the Low-Temperature Phase Transition of Tris(ethane-1,2-diamine)zinc(II) Dinitrate

Structural Definition of the Low-Temperature Phase Transition of Tris(ethane-1,2-diamine)zinc(II) Dinitrate

Electron Paramagnetic Resonance of Mn2+ in Orthorhombic and Higher Symmetry Crystals

EPR and optical properties of impurity centers in low-symmetry crystals

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Electron Paramagnetic Resonance of Mn²⁺ in Orthorhombic and Higher Symmetry Crystals