2011
DOI: 10.1007/978-1-4419-0643-4
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Computational Methods for Microstructure-Property Relationships

Abstract: Polycrystalline materials exhibit deformation patterns that are heterogeneous both between and within crystals. The deformation heterogeneity within crystals can arise from variations of the crystallographic slip due to spatial variations in the stress driven by interactions among neighboring crystals. Typically, misorientations develop across crystals if the slip is not homogeneous. Furthermore, dislocations may accumulate within crystals, causing lattice distortion (elastic straining) and contributing to the… Show more

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Cited by 51 publications
(3 citation statements)
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“…This is because these techniques provide micro-structural information that is quite valuable for a mechanistic interpretation of the failure. In this regard the use of FIB-SEM instrument with automated features has emerged to obtain multi-modal information in 3D using serial sectioning by applying the cross-section ion milling technique (usually Ga + ion sputtering) 52 The nature of information characterised in 3D could be the general microstructural features such as precipitates, grains, and damage such voids as well as orientation of grain and chemical mapping of elements. The imaging of the fine micro-structural features in the nano-meter scale visualised in 3D using voxel dimensions in tens of nano-meters can be characterised over typical volumes of about 1000 um 3 using FIB-SEM.…”
Section: Multi-modal and Multi-scale Characterisation Of Cavitation Imentioning
confidence: 99%
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“…This is because these techniques provide micro-structural information that is quite valuable for a mechanistic interpretation of the failure. In this regard the use of FIB-SEM instrument with automated features has emerged to obtain multi-modal information in 3D using serial sectioning by applying the cross-section ion milling technique (usually Ga + ion sputtering) 52 The nature of information characterised in 3D could be the general microstructural features such as precipitates, grains, and damage such voids as well as orientation of grain and chemical mapping of elements. The imaging of the fine micro-structural features in the nano-meter scale visualised in 3D using voxel dimensions in tens of nano-meters can be characterised over typical volumes of about 1000 um 3 using FIB-SEM.…”
Section: Multi-modal and Multi-scale Characterisation Of Cavitation Imentioning
confidence: 99%
“…In contrast the serial sectioning method to generate a 3D dataset presents a challenge to obtain the slices in their original form unscathed from the sputtering process 52 . Therefore careful optimisation of sputtering parameters to minimise material damage and its maintenance of these parameters over the long times (in the range of days) are quite critical to the success of the FIB-SEM to provide high -fidelity 3D dataset.…”
Section: Multi-modal and Multi-scale Characterisation Of Cavitation Imentioning
confidence: 99%
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