Abstract:The process of the epoxidation of cis,trans,trans-1,5,9-cyclododecatriene (CDT) to 1,2-epoxy-5,9-cyclododecadiene (ECDD) with the 30% aqueous hydrogen peroxide under the phase transfer conditions and with tert-butyl hydroperoxide under the homogeneous conditions was investigated. Onium salts such as Aliquat ® 336, Arquad ® 2HT, methyltrioctylammonium bromide and the Na 2 WO 4 /H 3 PO 4 catalyst system are very active under the phase transfer catalysis (PTC) conditions for the selective epoxidation of cis,trans… Show more
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