Comparison of the crystallisation and solid state reaction methods for the preparation of rare-earth orthophosphates

Bělina, Petr; Myšková, Veronika; Šulcová, Petra

doi:10.1007/s10973-009-0050-3

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Cited by 10 publications

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“…The syntheses were carried out by the standard solid-state reaction method [16][17][18][19][20]. The reagents in suitable weighed portions were homogenized by grinding in a mechanical agate mortar and then they were calcined in air atmosphere for several stages.…”

Section: Methodsmentioning

confidence: 99%

Phases in the subsolidus area of the system CuO–V2O5–Fe2O3

Blonska-Tabero

2012

J Therm Anal Calorim

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The phase equilibria in the solid state in the system FeVO 4 -Cu 3 V 2 O 8 and FeVO 4 -CuO have been determined. Based on the obtained DTA and XRD analysis results and some additional research, a phase diagram in the whole subsolidus area of the system CuO-V 2 O 5 -Fe 2 O 3 has been worked out. Eighteen subsidiary subsystems can be distinguished in this ternary system. Basic properties of the obtained phases with howardevansite-and lyonsite-type structure have been investigated by DTA, IR, and SEM methods.

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