1961
DOI: 10.1021/jo01064a641
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Communications- Preparation and Storage of Diphenylborinic Acid and Its Anhydride.

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1983
1983
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Cited by 32 publications
(13 citation statements)
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“…These compounds, which all contain a B-N bond, were obtained via the reaction of diphenylborinic acid with the corresponding α-amino acid (Fig. 2) rather than via the previously reported methods (Chremos et al, 1961;Flückiger et al, 1984;Farfán et al, 1993;Trujillo et al, 1998). The compounds (3a-j) were assayed using several different apoptotic indicator models, such as the inhibitory effect on cell growth measured by the MTT [3-(4,5-dimethylthiazo-2-yl)-2,5-diphenyl-tetrazolium bromide] assay, phosphatidylserine membrane externalization measured by Annexin V, and DNA distribution (sub-G 0 /G 1 peak) measured by PI staining, the last two using flow cytometry.…”
Section: Introductionmentioning
confidence: 99%
“…These compounds, which all contain a B-N bond, were obtained via the reaction of diphenylborinic acid with the corresponding α-amino acid (Fig. 2) rather than via the previously reported methods (Chremos et al, 1961;Flückiger et al, 1984;Farfán et al, 1993;Trujillo et al, 1998). The compounds (3a-j) were assayed using several different apoptotic indicator models, such as the inhibitory effect on cell growth measured by the MTT [3-(4,5-dimethylthiazo-2-yl)-2,5-diphenyl-tetrazolium bromide] assay, phosphatidylserine membrane externalization measured by Annexin V, and DNA distribution (sub-G 0 /G 1 peak) measured by PI staining, the last two using flow cytometry.…”
Section: Introductionmentioning
confidence: 99%
“…Solvents were used without further purification. The phenylborinic acid (Ph 2 BOH) was prepared in situ as previously reported in the literature . Melting points were determinate on an Electrothermal Mel‐Temp apparatus and are uncorrected.…”
Section: Methodsmentioning
confidence: 99%
“…Compounds I and 2 wcrc prcparetl by reacting thc appropriate aminoalcohol with an equimolar quantity ofdiphcnylborinic acid (obtained by acid hydrolysis of (2-aminoethanolnto)cliphenylboron) in ethanol/diethyl ether (6). A small amount of thc molecular complex 3 was isolated from thc reaction mixture during thc preparation of 2 as colorless crystals suitable for X-ray analysis.…”
Section: Methodsmentioning
confidence: 99%
“…Colorless crystals of 1 and 2 were obtained by rccsystallization from ethanol. Monoclinic, (1 = 9.6717 (13), b = 9.5867 (6). c = 14.452(2) A. P = 99.500 (7) tomcter.…”
Section: Methodsmentioning
confidence: 99%