1991
DOI: 10.1021/es00017a025
|View full text |Cite
|
Sign up to set email alerts
|

Comment on "Acid digestion for sediments, sludges, soils, and solid wastes. A proposed alternative to EPA SW 846 Method 3050"

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
1
1
1
1

Citation Types

1
10
0

Year Published

1992
1992
2022
2022

Publication Types

Select...
7
2

Relationship

0
9

Authors

Journals

citations
Cited by 16 publications
(11 citation statements)
references
References 4 publications
1
10
0
Order By: Relevance
“…Twenty-one ESPs were wiped with eight wet (DI H 2 O) PVC filters (26). These filters were allowed to dry at least 72 h, then weighed and chemically analyzed using a microwave digestion methodology, with modified parameters to increase the recovery of metal analytes (27,28). FBs were treated identically, where a wet PVC filter was used to wipe a clean ESP.…”
Section: Removing Particles From Esp and Filtersmentioning
confidence: 99%
“…Twenty-one ESPs were wiped with eight wet (DI H 2 O) PVC filters (26). These filters were allowed to dry at least 72 h, then weighed and chemically analyzed using a microwave digestion methodology, with modified parameters to increase the recovery of metal analytes (27,28). FBs were treated identically, where a wet PVC filter was used to wipe a clean ESP.…”
Section: Removing Particles From Esp and Filtersmentioning
confidence: 99%
“…13 35 The use of HCl as part of the digestion mixture is mandatory to solubilise Sb(V) as SbCl6and prevent Sb adsorption to silica material. 36 The use of HCl has the added advantage of dissolving common iron and silica minerals and apatite. 37 We have evaluated the use of HNO3-HCl mixtures for releasing Sb from mine contaminated sediments 38 and found Sb is nearly quantitatively extracted (using a 2:…”
Section: Biotamentioning
confidence: 99%
“…Treatment of antimony data in this report is incomplete for two reasons. First, digestions using only nitric acid are known to yield variable recoveries [24] and second, some of the analyses were performed by inductively coupled plasma-optical emission spectrometry (ICP-OES) and some by inductively coupled plasma-mass spectrometry (ICP-MS). The former had an antimony detection limit of approximately 20 mg kg À1 which was too high for most of these samples, rendering some of the comparisons problematic.…”
Section: Comparison Of Heterogeneity Of Distribution Of Small Arms Ramentioning
confidence: 99%