2013
DOI: 10.1063/1.4816257
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Columns formed by multiple twinning in nickel layers—An approach of grain boundary engineering by electrodeposition

Abstract: Complementary microscopic and diffraction based methods revealed a peculiar microstructure of electrodeposited nickel. For the as-deposited layer, thus, without any additional treatment, multiple twinning yields a high population of Σ3n boundaries, which interrupts the network of normal high angle grain boundaries. A peculiar arrangement of Σ3 boundaries forming five-fold junctions is observed. The resulting microstructure meets the requirements for grain boundary engineering. Twinning induced effects on the c… Show more

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Cited by 7 publications
(13 citation statements)
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“…Nickel films were deposited onto an amorphous substrate applying electrochemical deposition from a Watts bath with different amounts of the organic additive 2-butyne-1,4-diol and varying current densities; for details on electrodeposition the reader is referred to Alimadadi et al (2012). The thin amorphous substrate layer was deposited onto a copper sheet prior to the deposition of the nickel films.…”
Section: Thin-film Depositionmentioning
confidence: 99%
“…Nickel films were deposited onto an amorphous substrate applying electrochemical deposition from a Watts bath with different amounts of the organic additive 2-butyne-1,4-diol and varying current densities; for details on electrodeposition the reader is referred to Alimadadi et al (2012). The thin amorphous substrate layer was deposited onto a copper sheet prior to the deposition of the nickel films.…”
Section: Thin-film Depositionmentioning
confidence: 99%
“…3b). A map of this kind is known to visualize boundaries between small crystallites, though corresponding orientation map would not necessarily reveal them [27]. Actually, Fig.…”
Section: Resultsmentioning
confidence: 99%
“…2. Cross-sectional characterization of deposits using EBSD has previously been applied on various materials [29,30] including nickel [4,22,28]. However, microtexture information [31] is rarely obtained.…”
Section: Discussionmentioning
confidence: 99%
“…At a distance of 4 µm from the interface, the texture remains weak, although various components evolve. Further away from the interface a major <210> has developed, accompanied by two minor components, <542> and <711>, both originating from twinning of <210> [22]. This texture remains on further growth of the electrodeposit.…”
Section: Texture Evolutionmentioning
confidence: 99%
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