Chromatographic fingerprint, antioxidant activity, and colour characteristic of polish goldenrod (Solidago virgaurea L.) honey and flower

Jasicka-Misiak, Izabela; Makowicz, Ewa; Stanek, Natalia

doi:10.1007/s00217-018-3034-3

Cited by 39 publications

(57 citation statements)

References 33 publications

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“…Before the experiments, the fiber was conditioned according to the manufacturer's instructions. The details of the analysis procedure were described previously [17]. For analysis, 5 g of honey was dissolved in 5 mL of distilled water, and 0.75 g of NaCl was added.…”

Section: Headspace Solid-phase Microextraction (Hs-spme) Methodologymentioning

confidence: 99%

“…Ultrasound solvent extraction and solid-phase extraction were performed according to the procedures described previously [17][18][19]. For each honey sample, the extraction was performed in triplicate.…”

Section: Ultrasound-assisted Extraction (Uae) and Solid-phase Extractmentioning

confidence: 99%

“…High-performance thin-layer chromatography was used to analyze the lipophilic fractions obtained by UAE and SPE using the parameters developed in our laboratory [17,19]. Ten microliters of each extract at a concentration of 100 ± 5 ng/spot was applied to the plate in 10 mm bands 15 mm from the lower edge of the plate using a semiautomated HPTLC application device (Linomat 5, CAMAG, Muttenz, Switzerland) under a constant flow of nitrogen gas and at a rate of 250 nL•s −1 .…”

Section: Hptlc Separationmentioning

confidence: 99%

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Botanical Origin Authentication of Polish Phacelia Honey Using the Combination of Volatile Fraction Profiling by HS-SPME and Lipophilic Fraction Profiling by HPTLC

et al. 2019

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Eleven samples of Polish Phacelia tanacetifolia Benth., three Brassica napus and one Salix spp. honeys were characterized by melissopalynology and analysis of the compositions of their volatile fractions. Headspace solid-phase microextraction coupled with gas chromatography mass spectrometry (HS-SPME/GC-MS) using PDMS/CAR/DVB fiber was used for the isolation of low-molecular weight compounds which create a volatile fraction. To differentiate and indicate the most representative unifloral samples, chemometric techniques such as principal component analysis (PCA) and hierarchical-tree clustering (HTC) were applied to the dataset of the chromatographic fingerprints. Based on the obtained results, a unique chemical fingerprint of phacelia honey was generated. This study allows us to discriminate the botanical origin of the phacelia honeys based on the GC-MS and HPTLC analysis. In case of the GC-MS analysis trans-linalool oxide, hotrienol, cislinalool oxide and cis-epoxylinalool were identified as a predominant compound. Additionally lipophilic fractions obtained by ultrasound-assisted extraction (UAE) and solid-phase extraction (SPE) were subjected to the HPTLC analysis. It allowed the construction of a barcode-type identifier that could be used to differentiate the honey samples even without identifying the individual components of the obtained fraction.

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Section: Headspace Solid-phase Microextraction (Hs-spme) Methodologymentioning

confidence: 99%

Section: Ultrasound-assisted Extraction (Uae) and Solid-phase Extractmentioning

confidence: 99%

Section: Hptlc Separationmentioning

confidence: 99%

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Botanical Origin Authentication of Polish Phacelia Honey Using the Combination of Volatile Fraction Profiling by HS-SPME and Lipophilic Fraction Profiling by HPTLC

et al. 2019

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“…The naringenin glycoside naringin and the hesperetin glycoside hesperidin were the subjects of one study; however, they were not detected in aqueous or ethanolic S. virgaurea L. plant extracts . Another study described the components of goldenrod flowers in comparison with their originating honeys, but only naringenin was determined …”

Section: Introductionmentioning

confidence: 99%

“…21 Another study described the components of goldenrod flowers in comparison with their originating honeys, but only naringenin was determined. 22 For M. sativa L., as for S. virgaurea L. there are only a few publications. One study mentioned the presence of naringenin and hesperetin in lucerne, and another study mentioned the presence of liquiritigenin.…”

Section: Introductionmentioning

confidence: 99%

Flavonoids enantiomer distribution in different parts of goldenrod (Solidago virgaurea L.), lucerne (Medicago sativa L.) and phacelia (Phacelia tanacetifolia Benth.)

et al. 2019

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Plant material is a rich source of valuable compounds such as flavanones. Their different forms influence bioavailability and biological activity, causing problems with the selection of plant material for specific purposes. The purpose of this research was to determine selected flavanone (eriodictyol, naringenin, liquiritigenin, and hesperetin) enantiomer contents in free form and bonded to glycosides by an RP‐UHPLC‐ESI‐MS/MS method. Different parts (stems, leaves, and flowers) of goldenrod (Solidago virgaurea L.), lucerne (Medicago sativa L.), and phacelia (Phacelia tanacetifolia Benth.) were used. The highest content of eriodictyol was found in goldenrod flowers (13.1 μg/g), where it occurred mainly as the (S)‐enantiomer, and the greatest proportion of the total amount was bonded to glycosides. The richest source of naringenin was found to be lucerne leaves (4.7 μg/g), where it was mainly bonded to glycosides and with the (S)‐enantiomer as the dominant form. Liquiritigenin was determined only in lucerne, where the flowers contained the highest amount (1.2 μg/g), with the (R)‐enantiomer as dominant aglycone form and the (S)‐enantiomer as the dominant glycosylated form. The highest hesperetin content was determined in phacelia leaves (0.38 μg/g), where it was present in the form of a glycoside and only as the (S)‐enantiomer. A comparison of the different analyte forms occurring in different plant parts was performed for the first time.

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Characterization of Evodia rutaecarpa (Juss) Benth honey: volatile profile, odor‐active compounds and odor properties

Li,

Liu,

Shuai

et al. 2023

J Sci Food Agric

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BackgroundAroma is one of the most important quality criterion of different honeys and even defines their merchant value. The composition of volatile compounds, especially the characteristic odor‐active compounds, is an important contributor to honey aroma. Evodia rutaecarpa (Juss) Benth honey (ERBH) is a special honey in China with unique flavor characteristics. However, no work has yet been published in the literature to investigate the volatile compounds and characteristic odor‐active compounds of ERBHs. Therefore, it is necessary to systematically investigate the volatile profile, odor‐active compounds, and odor properties of ERBHs.ResultsThe characteristic fingerprint of ERBHs was successfully constructed with 12 characteristic peaks and a similarity range of 0.785‐0.975. A total of 298 volatile compounds were identified and relatively quantified by headspace solid‐phase microextraction (HS‐SPME) coupled with gas chromatography quadrupole time‐of‐flight mass spectrometry (GC‐QTOF), of which 61 and 31 were identified as odor‐active compounds by relative odor activity values (ROAVs) and GC‐olfactometry (GC‐O) analysis, respectively, especially the common 22 odor‐active compounds (E)‐β‐damascenone, phenethyl acetate, linalool, cis‐linalool oxide (furanoid), octanal, hotrienol, trans‐linalool oxide (furanoid), 4‐oxoisophorone, and eugenol, etc., contributed significantly to the aroma of ERBHs. The main odor properties of ERBHs was floral, followed by fruity, herbaceous, and woody aromas. The partial least‐squares regression (PLSR) results showed that the odor‐active compounds had good correlations with the odor properties.ConclusionIdentifying the aroma differences of different honeys is of great importance. This study provided a reliable theoretical basis for the quality and authenticity of ERBHs.This article is protected by copyright. All rights reserved.

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Chromatographic fingerprint, antioxidant activity, and colour characteristic of polish goldenrod (Solidago virgaurea L.) honey and flower

Cited by 39 publications

References 33 publications

Botanical Origin Authentication of Polish Phacelia Honey Using the Combination of Volatile Fraction Profiling by HS-SPME and Lipophilic Fraction Profiling by HPTLC

Botanical Origin Authentication of Polish Phacelia Honey Using the Combination of Volatile Fraction Profiling by HS-SPME and Lipophilic Fraction Profiling by HPTLC

Flavonoids enantiomer distribution in different parts of goldenrod (Solidago virgaurea L.), lucerne (Medicago sativa L.) and phacelia (Phacelia tanacetifolia Benth.)

Characterization of Evodia rutaecarpa (Juss) Benth honey: volatile profile, odor‐active compounds and odor properties

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