“…The Reaction of Cyclohexanone Azine with Cyanoacetic Acid-acetic Anhydride 1515 spirocyclic carbon atom resonated at 63.3 ppm and the corresponding carbon in 15 [12] resonated at 62.3 ppm ( Figure 5). The structure of 14 was confirmed by an X-ray analysis, the details of which are given in the Experimental Section and a Chem3D representation of the molecule is shown in Figure 6.…”
The reaction of cyclohexanone azine with a reagent produced by brief heating of cyanoacetic acid with acetic anhydride produced a highly substituted dihydropyrazolone.
“…The Reaction of Cyclohexanone Azine with Cyanoacetic Acid-acetic Anhydride 1515 spirocyclic carbon atom resonated at 63.3 ppm and the corresponding carbon in 15 [12] resonated at 62.3 ppm ( Figure 5). The structure of 14 was confirmed by an X-ray analysis, the details of which are given in the Experimental Section and a Chem3D representation of the molecule is shown in Figure 6.…”
The reaction of cyclohexanone azine with a reagent produced by brief heating of cyanoacetic acid with acetic anhydride produced a highly substituted dihydropyrazolone.
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