2010
DOI: 10.1002/chin.201101017
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ChemInform Abstract: The Topotactic Reduction of Sr3Fe2O5Cl2—Square Planar Fe(II) in an Extended Oxyhalide.

Abstract: Two unsymmetrical 1,2,4‐trithiolanes (1d and 1e) were reacted with [Pt0(PPh3)2(η2‐nbe)] (6; nbe=norborn‐2‐ene) and [Pt0(dppn)(η2‐nbe)] (11; dppn=1,8‐bis(diphenylphosphanyl)naphthalene)), respectively. Their treatment with compound 6 resulted in the formation of six‐membered platinacycles of type 7, which selectively underwent fragmentation into dithiolato complexes and thiobenzophenone (4b). The isolation of the first stable C‐substituted member of this class of compounds (i.e., compound 7e) permitted kinetic … Show more

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