“…Off‐white solid (EtOH‐dioxane); Mp = 183–185°C (lit. 184–185°C); IR (KBr): ν = 2220 (s) (CN), 1712 (s) (CO) cm −1 ; 1 H NMR (300 MHz, DMSO‐ d 6 ): δ 7.44–7.75 (m, 4H, Ar‐H), 8.30 (s, 1H, H4); 13 C NMR (75 MHz, DMSO‐ d 6 ): δ 103.61, 112.00, 117.56, 117.22, 128.15, 128.21, 136.50, 152.11, 155.20, 156.88. MS (EI, 70 eV): m/z = 171 [M + ], C 10 H 5 NO 2 : C, 70.18; H, 2.94; N, 8.18.…”