Chemischer Informationsdienst
 1972
DOI: 10.1002/chin.197241457
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ChemInform Abstract: STEROIDE 32. MITT. STEREOSPEZIFISCHE DARST. STICKSTOFFHALTIGER STEROIDE AUS AZIRIDINEN UND VICINALEN AZIDOALKOHOL‐METHANSULFONATEN

K. Ponsold1,
Dieter Klemm2

Abstract: Die Umsetzung der trans‐diaxialen Azido‐sulfonoxycholestane (I) bzw. (III) mit Na‐azid liefert die cis‐Diazide (IIa) (8 7% Ausbeute) bzw. (IVa) (70%), die mit Li‐alanat zu den cis‐Diaminen (IIb) bzw. (IVb) (isoliert als Hydrochloride; 44 bzw. 63%) reduziert werden.

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