Chemischer Informationsdienst
 1980
DOI: 10.1002/chin.198009034
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ChemInform Abstract: PREPARATION AND STRUCTURAL CHARACTERIZATION OF SALTS OF OXOTETRACHLOROTECHNETATE(V)

F. A. COTTON1,
Alan Davison2,
Victor W. Day3
et al.

Abstract: Reduktion des TeOz‐Ions mit H3PO2 in konz. wäßriger HCl‐Lösung liefert eine dunkelgrüne Lösung, aus der durch Zugabe großer Kationen wie Bu4N+ oder (Ph3P)2N+ grau‐grüne kristalline Festkörper mit dem Anion TeOCl; isoliert werden können (beim Bu4N ‐Salz 70% Ausb.).

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