Abstract:Iron I 7100 Mild Hydrothermal Synthesis, Crystal Structure, Thermal Behavior, Spectroscopic and Magnetic Properties of the (NH 4 )[Fe(AsO 4 ) 1-x (PO 4 ) x F] (I) (x = 0.3, 0.6, 0.8) Series. Thermal Transformation of (NH4)[Fe(AsO4)0.7(PO4)0.3F] into the Textural Porous Orthorhombic Fe(AsO4)0.7(PO4)0.3 (II). -Light-green single crystals of compounds (I) (orthorhombic space group Pna21 with Z = 8) are hydrothermally prepared from a mixture of Fe2(SO4)3, As2O5, H3PO4, HF, and NH4OH in H2O (autoclave, pH 3, 170°C,… Show more
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