ChemInform Abstract: K4Ni3O6 and KNa2Ni2O4, New Quasi One‐Dimensional Oxonickelates(II, III).

Đuriš, Katarina; Nuss, Juergen; Jansen, Martin

doi:10.1002/chin.201408008

ChemInform

2014

DOI: 10.1002/chin.201408008

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ChemInform Abstract: K₄Ni₃O₆ and KNa₂Ni₂O₄, New Quasi One‐Dimensional Oxonickelates(II, III).

Katarina Đuriš¹,

Juergen Nuss²,

Martin Jansen³

Abstract: K4Ni3O6 (I) and KNa2Ni2O4 (II) are obtained by the azide/nitrate route starting from stoichiometric mixtures of KN3, KNO3, NaN3, NaNO3, and NiO (Ag crucible, complex heating schedule, annealing at 873 K, 30 h (I) and 500 h (II)) followed by oxidation at 873 K (15 h (I) and 100 h (II)).

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ChemInform Abstract: K₄Ni₃O₆ and KNa₂Ni₂O₄, New Quasi One‐Dimensional Oxonickelates(II, III).

Abstract: K4Ni3O6 (I) and KNa2Ni2O4 (II) are obtained by the azide/nitrate route starting from stoichiometric mixtures of KN3, KNO3, NaN3, NaNO3, and NiO (Ag crucible, complex heating schedule, annealing at 873 K, 30 h (I) and 500 h (II)) followed by oxidation at 873 K (15 h (I) and 100 h (II)).

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