1994
DOI: 10.1002/chin.199446207
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ChemInform Abstract: Electrophilic Cyclization of α‐Terpineol in the Presence of Tl(O‐ OC‐CF3)3

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“…A decalona 45 foi preparada da octalona 40 (0,139 g; 0,78 mmol), Li (0,02 g), amônia (30 mL), t-BuOH (0,07 mL) e éter (2 mL) usando o procedimento descrito no item 5.2.1.9, exceto que a purificação foi realizada por coluna cromatográfica (sílica gel 70-230 Mesh; eluente: hexano/acetato de etila 7/3). Rendimento: 73% (0,103 g; 0,57 mmol).…”
Section: 2112preparação Da Trans-410-dimetil-trans-2-decalona (unclassified
“…A decalona 45 foi preparada da octalona 40 (0,139 g; 0,78 mmol), Li (0,02 g), amônia (30 mL), t-BuOH (0,07 mL) e éter (2 mL) usando o procedimento descrito no item 5.2.1.9, exceto que a purificação foi realizada por coluna cromatográfica (sílica gel 70-230 Mesh; eluente: hexano/acetato de etila 7/3). Rendimento: 73% (0,103 g; 0,57 mmol).…”
Section: 2112preparação Da Trans-410-dimetil-trans-2-decalona (unclassified