Abstract:Trialkylphosphite (I) reagieren mit Säurechloriden (II) zu den Acylderivaten (III), an die in Gegenwart von Dibutylamin als Base und unter Verwendung der leicht auskristallisierenden Methylester die Dialkylphosphite (IV) unter Bildung von Tetramethyl‐alkan‐1‐hydroxy‐1,1‐diphosphonaten (V) addiert werden.
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