Chemical Components of Atractylodes japonica Rhizome Oil

Chang, Kyung‐Mi; Kim, Gun-Hee

doi:10.3746/jfn.2010.15.2.147

Cited by 3 publications

(2 citation statements)

References 18 publications

(18 reference statements)

Supporting

Mentioning

Contrasting

Order By: Relevance

“…Sesquiterpenes and volatile compounds have been determined in A. macrocephala and A. lancea by GC coupled to flame ionization detector (FID) and MS, respectively . A. japonica ’s chemical content was also investigated by GC–MS . However, there are not enough chromatographic comparative analyses between baizhu and cangzhu's chemical composition.…”

Section: Introductionmentioning

confidence: 99%

Classification of the medicinal plants of the genus Atractylodes using high‐performance liquid chromatography with diode array and tandem mass spectrometry detection combined with multivariate statistical analysis

Cho

Kim

Suh

et al. 2016

J of Separation Science

View full text Add to dashboard Cite

Analytical methods using high-performance liquid chromatography with diode array and tandem mass spectrometry detection were developed for the discrimination of the rhizomes of four Atractylodes medicinal plants: A. japonica, A. macrocephala, A. chinensis, and A. lancea. A quantitative study was performed, selecting five bioactive components, including atractylenolide I, II, III, eudesma-4(14),7(11)-dien-8-one and atractylodin, on twenty-six Atractylodes samples of various origins. Sample extraction was optimized to sonication with 80% methanol for 40 min at room temperature. High-performance liquid chromatography with diode array detection was established using a C18 column with a water/acetonitrile gradient system at a flow rate of 1.0 mL/min, and the detection wavelength was set at 236 nm. Liquid chromatography with tandem mass spectrometry was applied to certify the reliability of the quantitative results. The developed methods were validated by ensuring specificity, linearity, limit of quantification, accuracy, precision, recovery, robustness, and stability. Results showed that cangzhu contained higher amounts of atractylenolide I and atractylodin than baizhu, and especially atractylodin contents showed the greatest variation between baizhu and cangzhu. Multivariate statistical analysis, such as principal component analysis and hierarchical cluster analysis, were also employed for further classification of the Atractylodes plants. The established method was suitable for quality control of the Atractylodes plants.

show abstract

Section: Introductionmentioning

confidence: 99%

Classification of the medicinal plants of the genus Atractylodes using high‐performance liquid chromatography with diode array and tandem mass spectrometry detection combined with multivariate statistical analysis

Cho

Kim

Suh

et al. 2016

J of Separation Science

View full text Add to dashboard Cite

show abstract

“…Camphor is a saturated ketone containing a camphene skeleton and is obtained industrially via pinene, camphene, and isoborneol ( 29 ). Camphor was initially characterized in Eclipta prostrata L. and Atractylodes japonica PEOs in small amounts ( 30 , 31 ). Four esters (2.59%), ( E )-sabinene hydrate, bornyl acetate, sabinyl acetate, and α-terpinyl acetate, were found in C. zawadskii var.…”

Section: Resultsmentioning

confidence: 99%

Volatiles of Chrysanthemum zawadskii var. latilobum K.

Chang¹,

Kim²

2012

JFN

Self Cite

View full text Add to dashboard Cite

The volatile aroma constituents of Chrysanthemum zawadskii var. latilobum K. were separated by hydro distillation extraction (HDE) method using a Clevenger-type apparatus, and analyzed by gas chromatography-mass spectrometry (GC/MS). The yield of C. zawadskii var. latilobum K. flower essential oil (FEO) was 0.12% (w/w) and the color was light green. Fifty-five volatile chemical components, which make up 88.38% of the total aroma composition, were tentatively characterized. C. zawadskii var. latilobum K. FEOs contained 27 hydrocarbons, 12 alcohols, 7 ketones, 4 esters, 1 aldehyde, 1 amine, and 3 miscellaneous components. The major functional groups were terpene alcohol and ketone. Borneol (12.96), (±)-7-epi-amiteol (12.60), and camphor (10.54%) were the predominant volatiles. These compounds can be used in food and pharmaceutical industries due to their active bio-functional properties.

show abstract