2006
DOI: 10.1524/zpch.2006.220.2.153
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Characterization of the Grain Size in Ferromagnetic Colloids: Comparing Torsional-Pendulum Measurements with Standard Complementary Methods

Abstract: Ferrofluids / Particle Size Analysis / Relaxation TimeA recently introduced shear-flow-free method for measuring the rotational viscosity of a resonantly forced torsional pendulum is used to determine the transverse magnetic relaxation time in magnetite and cobalt-based ferrofluids. From these data the average size of the ferromagnetic grains and their hydrodynamic diameter (core plus surfactant coating) are deduced under in-situ conditions, i.e. without diluting the sample. The reliability of the method is de… Show more

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Cited by 13 publications
(11 citation statements)
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“…N°F 083094CX from Ferrotec, Co.͒ which contains magnetite particles stabilized in synthetic hydrocarbon by a surfactant. The data were fitted according to Embs et al 15 by The same is true for the critical induction of the Rosensweig instability in the ferrofluid, affected sensitively by these parameters.…”
Section: A Materialsmentioning
confidence: 99%
“…N°F 083094CX from Ferrotec, Co.͒ which contains magnetite particles stabilized in synthetic hydrocarbon by a surfactant. The data were fitted according to Embs et al 15 by The same is true for the critical induction of the Rosensweig instability in the ferrofluid, affected sensitively by these parameters.…”
Section: A Materialsmentioning
confidence: 99%
“…[308] Other techniques include magneto-granulometry, photon correlation spectroscopy, Raman spectroscopy, and torsional pendulum measurements. [216,309] Vibrational spectroscopy is also a powerful tool for studying the fundamental properties of magnetic oxides. The finite scale length effect for CoFe 2 O 4 inverse spinel MNPs was studied from infrared vibrational properties by observing the strong magnetoelastic coupling.…”
Section: Characterization Techniquesmentioning
confidence: 99%
“…For our calculations we use typical values of the parameters [25][26][27][28] that characterize the ferrofluid APG933 of FerroTec: M sat mat 450 kA/m, = 4.1%, ρν = 0.5 Pa s, s = 2 nm, f 0 = 10 9 Hz, and K = 15 kJ/m 3 . The equilibrium magnetization M eq (H ) of APG933 is obtained with a polydisperse fit to experimental data that is described in detail in Ref.…”
Section: A Ferrofluid Parametersmentioning
confidence: 99%