2023
DOI: 10.1016/j.polymer.2023.126203
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Characterisation of micro polymer inclusion beads by thermogravimetric analysis

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Cited by 6 publications
(2 citation statements)
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“…TGA was conducted to further detect the thermal stability of each PVDF-HFP-matrix electrolyte membrane, as shown in Figure c. TGA thermogram of pure PVDF-HFP-F membrane reflects no signs of degradation until 460 °C, but it has a single-step rapid weight loss due to pyrolysis of the PVDF-HFP backbones and almost no residual solvent in this sample . Both PPA x samples start to degrade at lower temperatures than the pristine membrane and have different decomposition stages because the introduced copolymer plasticizers deteriorate their thermal stabilities.…”
Section: Resultsmentioning
confidence: 99%
“…TGA was conducted to further detect the thermal stability of each PVDF-HFP-matrix electrolyte membrane, as shown in Figure c. TGA thermogram of pure PVDF-HFP-F membrane reflects no signs of degradation until 460 °C, but it has a single-step rapid weight loss due to pyrolysis of the PVDF-HFP backbones and almost no residual solvent in this sample . Both PPA x samples start to degrade at lower temperatures than the pristine membrane and have different decomposition stages because the introduced copolymer plasticizers deteriorate their thermal stabilities.…”
Section: Resultsmentioning
confidence: 99%
“…However, in the case of µPIBs, additional acidification of the NaCl desolvation and delivery solutions was necessary to prevent D 2 EHPA carrier leaching. In subsequent research, Croft et al [74], while characterizing micro polymer inclusion beads using thermogravimetric analysis, discovered, inter alia, that the presence of Na + in both PVC and PVDF-HFP based µPIBs negatively influenced the extraction efficiency of La(III) ions. In that study, they also found that this adverse process can be prevented, e.g., by washing the µPIBs with 1 M sulfuric acid after their formulation to remove the undesirable Na + ions.…”
Section: Polymer Inclusion Membranes In the Recovery Of Reesmentioning
confidence: 99%