2004
DOI: 10.6028/nist.sp.260-156
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Certification of NIST Standard Reference Material 1575a pine needles and results of an international laboratory comparison

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Cited by 13 publications
(8 citation statements)
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“…Calcium and sodium values for NIST-1547 by INAA have not been reported in recent publications [32,33]. Sodium results from the latest re-assessment of this SRM by NIST itself were in agreement [34], even if such an agreement may be viewed as somewhat arguable since the uncertainty is around 40% ðNa : 25:7 AE 10Þ. The results from ITN and TUDelft concur with the latter, due account made for their ranges of uncertainty.…”
Section: Resultssupporting
confidence: 76%
“…Calcium and sodium values for NIST-1547 by INAA have not been reported in recent publications [32,33]. Sodium results from the latest re-assessment of this SRM by NIST itself were in agreement [34], even if such an agreement may be viewed as somewhat arguable since the uncertainty is around 40% ðNa : 25:7 AE 10Þ. The results from ITN and TUDelft concur with the latter, due account made for their ranges of uncertainty.…”
Section: Resultssupporting
confidence: 76%
“…In particular, before the determination of chemical elements, samples (125 mg each) were subjected to microwave mineralization in a Milestone Microwave Laboratory System (mls 1200, Shelton, CT, USA) by a combination of 50% HF and 65% HNO 3 (1:2 = v:v), and deionized water. Standard Reference Material was used to evaluate the analytical accuracy [41]. Indications on the pH values of the biodeposits were obtained in situ with litmus papers (range 0–14).…”
Section: Methodsmentioning
confidence: 99%
“…There is a tradition of innovation in measurement science to characterize these high-impact samples 1 . New technologies are used, rigorous experimental designs are employed, and exotic methods applied 2 , 3 . In a virtuous cycle, existing methods are optimized and new methods are developed using reference materials as the benchmarks.…”
Section: Background and Summarymentioning
confidence: 99%