“…The recrystallized material was kept in desiccators for drying. FAB positive: 874, 1 H-NMR (DMSO-d 6 ): δ = 6.74 (s, 8H, ArH) 4.22 (d, 4H, J = 12Hz, Ar-CH 2 -Ar), 3.14 (d, 4H, J = 12Hz, Ar-CH 2 -Ar) 3.10 (s, 8H, ArCH 2 N), 2.26 (br s, 32H, NCH 2 CH 2 N), 2.12(s, 24H, NCH 3 )…”