Biiyukyilmaz T, Sen BH, Bgaard B. Retention of titanium tetrafluoride (Ti,), used as ffisure sealant on human deciduous molars. Acta Odontol Scand 1997;55:73-78. Oslo. ISSN 00014357. When dental hard tissues are exposed to aqueous solutions of TiF4, an acid-resistant glaze forms on tooth surfaces. The aim of the present study was to examine the long-term retention of the glaze on TiF4-treated deciduous molars. The occlusal surfaces of four deciduous molars in each of Seven children were treated with 4% TiF, for 1 min. The sealed teeth were extracted after 1, 3, 6, or 12 months and examined with scanning electron microscopy. An extensive surface layer was present on all deciduous molars after I month. After 3 months the glaze appeared to be worn out on the cusp tips and in some a r e a on the cusp inclines. At 6 months the glaze was observed as small areas distributed over the cusp inclines with total coverage of the pits and fwures. After 1 year the presence of the glaze was limited to pits and fissures.