Capillary gas chromatographic — Mass spectrometric determination of iprodione in chicory and leek

Determination and validation of a simple high-performance liquid chromatographic method for simultaneous assay of iprodione and vinclozolin in human urine

“…The filtration of extracts before injection onto chromatographic column avoids rapid obstruction of the precolumn, increasing its life. The main advantage of this method in comparison with previous papers report in literature [28,29] is the rapid SPE procedure for the preparation of the biological sample, which gives high extraction yields. The proposed HPLC method employing solid-phase extraction for sample preparation is simple and convenient for the determination of iprodione and vinclozolin in urine samples.…”

“…Methods used to analyse fungicides and their residues are similar to those used for other pesticides. Gas chromatography (GC) is a classical method, and presently GC-MS is often used [16][17][18][19] and liquid chromatography (LC) is more widely recommended for thermally and unstable labile compounds, usually in conjunction with UV, fluorimetric detection or with a mass spectrometry system [20][21][22][23][24][25][26][27][28]. Rodriguez of fungicides from vegetables [29].…”