Calorimetry of 4-aminopyridine

Abstract

Signature was redacted for privacy. Signature was redacted for privacy. Signature was redacted for privacy. V 2. Experimental 225 a. Preparation of KCl(s) 225 b. Injection of KCl(s) Into H^O 226 3. Results and discussion 228 B. Heat of Neutralization for Reaction of 230 NaOH(aq) and HClO^(aq) 1. History 230 2. Experimental a. Preparation of solution b. Standardization of solutions c. Thermometric titration of NaOH(aq) with HClO^ 3. Results and discussion 239 VIII. INVESTIGATION OF 4-AMINOPYRIDINE AS A 260 CALORIMETRIC STANDARD 3. Thermometric titration of 264 4-amlnopyrldine(aq) with HClO^(aq) 4. Preparation of 4-aminopyridine 264 perchlorate(s) 5. Spectral properties of 266 4-aminopyrldine(s) and 4-amlnopyrldlne perchlorate(s) 6. Thermal properties of 266 4-amlnopyrldine(s) and 4-amlnopyrldine perchlorate(s) vl C. Results and Discussion 26? 1. Purity and properties of 26? 4-aininopyridlne (s) and 4-aminopyridlne perchlorate(s) 2. Heat of solution of 4-aininopyridine(s) 3. Heat of neutralization of 277 4-aminopyridine(aq) with HClO^(aq)