Abstract:An undergraduate laboratory experiment
for the synthesis of biologically
significant bis-4-hydroxycoumarins using a new catalyst is described
here. An experimental setup plan, monitoring the reaction by TLC,
isolation of the product, safe laboratory handling procedures, and
significance of data reproducibility of the result are the main learning
outcomes of this work. The products are characterized by melting point, 1H nuclear magnetic resonance (NMR), 13C NMR, distortion
enhancement by polarization transfer … Show more
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