1992
DOI: 10.1142/s0129083592000348
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Bio-PIXE AT THE TAKIZAWA FACILITY (Bio-PIXE WITH A BABY CYCLOTRON)

Abstract: For the developement of bio-PIXE, two problems remain to be solved; one in accelerator availability and the other in data analysis. To improve the former, a method of applying baby cyclotrons to PIXE has been developed. To solve the latter, the computer program SAPIX for x-ray spectrum analysis ,which runs on ordinary personal computers and is fairly easy to operate has been developed. Examples of spectral fitting by the SAPIX and a description of the program are given. Further, the two-detector measuring syst… Show more

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Cited by 178 publications
(35 citation statements)
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“…About 15 cm 2 of each sample was crushed to a fine powder with a powder mill (Varian PM-2005m, Osaka Chemical Co., Ltd., Osaka, Japan) to produce homogeneous samples for analysis. The tree bark powders (30 mg of each sample) were digested with a mixture of indium (In) and HNO 3 in a ratio of 3:100, before the heavy metal concentrations such as Pb, Zn, Fe (especially Hg), and As were determined with PIXE [19,20] at Iwate Medical University (Iwate, Japan). The dimensions of the tree bark samples (about 15 cm 2 ) were calculated with the ImageJ (version 1.48) software (National Institutes of Health, Bethesda, MD, USA).…”
Section: Sample Preparationmentioning
confidence: 99%
“…About 15 cm 2 of each sample was crushed to a fine powder with a powder mill (Varian PM-2005m, Osaka Chemical Co., Ltd., Osaka, Japan) to produce homogeneous samples for analysis. The tree bark powders (30 mg of each sample) were digested with a mixture of indium (In) and HNO 3 in a ratio of 3:100, before the heavy metal concentrations such as Pb, Zn, Fe (especially Hg), and As were determined with PIXE [19,20] at Iwate Medical University (Iwate, Japan). The dimensions of the tree bark samples (about 15 cm 2 ) were calculated with the ImageJ (version 1.48) software (National Institutes of Health, Bethesda, MD, USA).…”
Section: Sample Preparationmentioning
confidence: 99%
“…Once dry, the samples were crushed to fine powder using a powder mill (Varian PM-2005 m, Osaka Chemical Co., Ltd, Osaka, Japan). The shoot powder (30 mg of each sample) was digested with a mixture of In:HNO 3 at a ratio of 3:100 before determination of the heavy metal concentrations by particle induced X-ray emission (PIXE) [17] at Cyclotron Center of Iwate Medical University, Iwate, Japan. Then, 20 mg of both the roots and shoots were digested with a solution of H 2 O 2 , HF, and HNO 3 at a ratio of 2:5:10 before heavy metal concentrations were determined by inductively coupled plasma-optical emission spectrometry (ICP-OES) (Varian Optima TM 8300 series, PerkinElmer, Kanagawa, Japan) at the Integrated Centre for Sciences, Ehime University, Matsuyama, Japan.…”
Section: Methodsmentioning
confidence: 99%
“…The analytical conditions followed Sera et al (1992) [26]. A small cyclotron provides a 2.9 MeV-proton beam on the target after passing through a beam collimator of graphite.…”
Section: Methodsmentioning
confidence: 99%