The spectra of gamma radiation following pile-neutron capture in separated isotopes of nickel have been measured with a three-crystal scintillation pair spectrometer as well as with a single-crystal scintillation counter. Energies and intensities of the gamma rays from each isotope are reported. Each of the lines observed with natural nickel has been assigned to Ni 58 (^,7)Ni^, Ni 60 (w,Y)Ni 61 , or Ni 62 (#,Y)Ni 63 . In some cases, gamma rays of nearly identical energies are found in two, or in all three, isotopes. Additional gamma rays not resolved in the natural nickel spectrum appear in Ni 58 (#,y)Ni 59 at 7.65 Mev, and in Ni 60 (w,y)Ni 61 at 7.65 Mev, and in Ni 60 (w,7)Ni 61 at 4.70 and 5.55 Mev. The spectrum of Ni 62 (w,r)Ni 63 is dominated by a strong line at 6.80 Mev, presumably the ground -state transition.