2021
DOI: 10.26434/chemrxiv.14439773.v1
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Sijing Xue,
Bart Limburg,
Debasish Ghorai
et al.

Abstract: Dual palladium/photoredox-catalysis provides an effective method for the asymmetric synthesis of vicinal a,b-tri/tetra- or a,b-tetra-substituted homoallylic alcohols. Regio- and enantioselective decarboxylative allylic alkylation of vinyl cyclic carbonates is reported using Hantzsch type esters as radical precursors. The developed methodology combines the use of versatile and accessible reagents and can be operated under mild reaction conditions giving the target molecules in appreciable to good yields, high b…

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