Asymmetric photosensitized addition of methanol to (R)-(+)-(Z)-limonene in a microreactor

Sakeda, Kosaku; Wakabayashi, Kazuhito; Matsushita, Yasuyuki; Ichimura, Teijiro; Suzuki, Tadashi; Wada, Takehiko; Inoue, Yoshihisa

doi:10.1016/j.jphotochem.2007.05.019

Cited by 42 publications

(11 citation statements)

References 21 publications

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“…The reaction was performed in a quartz microreactor; however, the reaction suffered from poor product selectivity and d.e. Comparison with a batch reactor showed that the batch reactor gave much higher conversion [50,69]. Subsequent work has shown that the conversion of this reaction in a microflow reactor can be improved through the use of high-power, high-pressure Hg lamps [28].…”

Section: Reviewmentioning

confidence: 99%

Flow photochemistry: Old light through new windows

Knowles

Elliott²,

Booker‐Milburn³

2012

Beilstein J. Org. Chem.

367

190

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SummarySynthetic photochemistry carried out in classic batch reactors has, for over half a century, proved to be a powerful but under-utilised technique in general organic synthesis. Recent developments in flow photochemistry have the potential to allow this technique to be applied in a more mainstream setting. This review highlights the use of flow reactors in organic photochemistry, allowing a comparison of the various reactor types to be made.

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Section: Reviewmentioning

confidence: 99%

Flow photochemistry: Old light through new windows

Knowles

Elliott²,

Booker‐Milburn³

2012

Beilstein J. Org. Chem.

367

190

View full text Add to dashboard Cite

show abstract

“…The formation of photoproducts increases with longer irradiation and the trans -product is formed in excess of the cis -product. A quartz microreactor with ultraviolet (UV) irradiation was used for this reaction [25] .…”

Section: Photochemical Asymmetric Reactionsmentioning

confidence: 99%

Asymmetric Reactions in Flow Reactors

Rasheed

Elmore

Wirth

2011

Catalytic Methods in Asymmetric Synthesis

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“…We reexamined the two asymmetric photosensitized reactions in a microreactor [24]. Numerous efforts have been made to develop various methodologies for asymmetric chemical synthesis.…”

Section: Asymmetric Photosensitized Reactions In Microreactorsmentioning

confidence: 99%