“…Several methods use electrolytically generated silver ions to precipitate the chloride. The chloride concentration is determined from the amount of solution and the voltage and current versus time curves (Blaedel, 1952;Marinenko, 1963;Masten, 1954;Peters, 1969;Shiner, 1956;Stern, 1958). Mercury electrodes may be used similarly (DeFord, 1956;Przybylowicz, 1956).…”
“…Several methods use electrolytically generated silver ions to precipitate the chloride. The chloride concentration is determined from the amount of solution and the voltage and current versus time curves (Blaedel, 1952;Marinenko, 1963;Masten, 1954;Peters, 1969;Shiner, 1956;Stern, 1958). Mercury electrodes may be used similarly (DeFord, 1956;Przybylowicz, 1956).…”
“…It has been thoroughly studied by several investigators (3,5,18,25,33,44) and the principle explained in terms of polarization and depolarization. Kolthoff (36) and Duyckaerts (8) have recently given excellent comparisons between various closely related techniques.…”
Square wave titrimetry has been applied to redox, precipitation, and complex formation reactions, lodinearsenite, ferrous-cerium(IV), and ferrocyanide-cerium(IV) reactions gave successful titrations. Equimolar mixtures
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