Application of Lavender-Oil Microcapsules to Functionalized PET Fibers

Abstract

Surface treatments for textile substrates have received significant attention from researchers around the world. Ozone and plasma treatments trigger a series of surface alterations in textile substrates that can improve the anchoring of other molecules or particles on these substrates. This work aims to evaluate the effect of ozone and plasma treatments on the impregnation of polymeric microcapsules containing lavender oil in polyester fabrics (PES). Microcapsules with walls of chitosan and gum arabic were prepared by complex coacervation and impregnated in PES, plasma-treated PES, and ozone-treated PES by padding. The microcapsules were characterized for their size and morphology and the surface-treated PES was evaluated by FTIR, TGA, SEM, and lavender release. The microcapsules were spherical in shape, with smooth surfaces. The FTIR analyses of the textile substrates with microcapsules showed bands referring to the polymers of the microcapsules, but not to the lavender; this was most likely because the smooth surface of the outer wall did not retain the lavender. The mass loss and the degradation temperatures measured by TGA were similar for all the ozone-treated and plasma-treated polyester samples. In the SEM images, spherical microcapsules and the impregnation of the microcapsules of larger sizes were perceived. Through the lavender release, it was observed that the plasma and ozone treatments interfered both with the amount of lavender delivered and with the control of the delivery.

Preparation and characterisation of microcapsules loaded with essential oils (eucalyptus, aloe vera and lavender): encapsulation of cotton woven fabric and evaluation

“…The TGA outcome showed that the initial mass loss occurred at 280 o C. Furthermore, the greatest rate of weight loss was noted between 281-394°C, which is related to the cellulose's degradation. The encapsulated cotton fabric's (C1, C5, C7, C8, C13) TG curve showed a lower temperature of disintegration, with the greatest rate of weight decrease occurring between 234°C and 394°C (Valle et al 2023). The decomposition temperature and mass loss are shown in Fig.…”