Air-breathing propulsion has the ability to provide more economical access-to-space than current rocket based systems. Access-to-space requires hypersonic flight within the atmosphere, the air-breathing cycle best suited to this is the scramjet. Next generation launch systems require a scramjet stage to operate into the hypervelocity regime (> 3 km/s). Performance data at these conditions is scarce due to the inability of ground test facilities to replicate the high total pressures and temperatures associated with flight. Also, flight experiments are subject to material limitations and are generally prohibitively expensive. This thesis details experiments which add to the currently limited data-set of scramjet performance at hypervelocity conditions.The Mach 12 rectangular-to-elliptical shape-transitioning (RESTM12) engine is currently under investigation at The University of Queensland as a potential candidate for access-to-space. The RESTM12 engine is designed to accelerate from Mach 6-12 as a part of a rocket-scramjet-rocket access-to-space system. Previous testing of the RESTM12 engine has shown good performance at off-design conditions and now as a result of this investigation, robust performance at its design condition.The primary aim of this thesis was to:"investigate experimentally whether robust supersonic combustion can be generated in a three-dimensional scramjet flowpath at a Mach 12 flight condition in an impulse facility."In order to achieve this two experimental campaigns where undertaken in the T4 Stalker Tube. Both experiments used the facilities Mach 10 nozzle to generate a test flow equivalent to Mach 11.8 flight at 38.3 km altitude. Initial experiments investigating hypervelocity boundary layer transition showed that natural transition would not occur in a length equivalent to the forebody and inlet of the engine. The ingestion of a laminar boundary layer into the inlet of the RESTM12 engine would increase the likelihood of developing a separation in the inlet that would not allow it to operate as intended. To reduce the susceptibility of the inlet to separation a boundary layer trip was required.i Based on the Hyper-X program's boundary layer trip development experiments (Berry et al., 2001a), several combinations of trip geometry, height and location were tested on a flat plate model resulting in a successful trip configuration. Now confident that a trip configuration capable of providing the RESTM12 engine with a turbulent boundary layer was designed, the engine was tested at its design condition.A half-scale model of the RESTM12 scramjet engine was tested in a semi-free-jet configuration utilising both inlet and step injection of gaseous hydrogen fuel. Once it was established that the inlet was operating correctly and sufficient test time was available the experiments began with fuel injection. Initial tests showed that robust combustion occurred when inlet injection was employed. The most successful fuelling configuration was a combined injection scheme where 31% of the fuel was ...