Abstract:High free fatty acid (FFA) content results in low palm oil yield in refinery and 5 wt% are the limit for crude palm oil acceptance. Common method of the FFA quantification in the mills is titration. The intent of this study was to determine the FFA content in extracted palm oil by using Fourier transform infrared (FTIR) spectroscopy coupled with AOCS titration method for verification. The oil extractions took place on days 1, 5, 8, 12 and 15. The fruitlets were initially washed and autoclaved. By separating th… Show more
“…According to Beer's Lambert Law, the absorbance is directly proportional to the concentration. Thus, as carbonyl double bonds, C = O stretch increased, the absorbance also increased indicating higher free fatty acid content in the oil sample [26].…”
Palm oil is an <span>edible vegetable oil yielded from the mesocarp of the palm oil’s fruit. It is commonly used as cooking oil as compared to other cooking oil such as olive or coconut oil because it is inexpensive and has high oxidative stability when used for frying. However, after frequent frying, the oil undergoes some physical and chemical reactions which affect the quality. This leads to the formation of compound that is dangerous to human body which is called free fatty acid (FFA). Therefore, a measurement device needs to be developed to determine the quality of heated cooking oil. In this paper, a spectroscopy study using an open-path method which focus on the palm cooking oil is proposed to examine the reaction of palm oil upon prolonged heating process. Open-path method is a technique where the incident beam will travel through the sample (palm oil) before it is detected by a spectrometer. The result shows that the FFA samples have the optimum absorbance peak at the UV wavelength 339.15 nm and each prolonged heated oil show different absorbance value. Hence, there is a potential to develop an optical sensor to determine the quality of the heated cooking oil.</span>
“…According to Beer's Lambert Law, the absorbance is directly proportional to the concentration. Thus, as carbonyl double bonds, C = O stretch increased, the absorbance also increased indicating higher free fatty acid content in the oil sample [26].…”
Palm oil is an <span>edible vegetable oil yielded from the mesocarp of the palm oil’s fruit. It is commonly used as cooking oil as compared to other cooking oil such as olive or coconut oil because it is inexpensive and has high oxidative stability when used for frying. However, after frequent frying, the oil undergoes some physical and chemical reactions which affect the quality. This leads to the formation of compound that is dangerous to human body which is called free fatty acid (FFA). Therefore, a measurement device needs to be developed to determine the quality of heated cooking oil. In this paper, a spectroscopy study using an open-path method which focus on the palm cooking oil is proposed to examine the reaction of palm oil upon prolonged heating process. Open-path method is a technique where the incident beam will travel through the sample (palm oil) before it is detected by a spectrometer. The result shows that the FFA samples have the optimum absorbance peak at the UV wavelength 339.15 nm and each prolonged heated oil show different absorbance value. Hence, there is a potential to develop an optical sensor to determine the quality of the heated cooking oil.</span>
“…FFA is a parameter that determines the quality of CPO; if the level of FFA is high, then the quality of CPO is low and vice versa. The formation of FFA will quickly occur if the fruit is damaged, loose, over ripe or contain R S Handayani 1 *, N Bachri 2 , R Rusydi [7]. The effort that can be done to prevent fruit damage is through spraying a solution of calcium chloride and sodium benzoate.…”
Palm oil yields are often of low quality and quantity. Production quality improvement can be done by preventing damaged or defective products, for example by spraying a solution of calcium chloride and sodium benzoate. This research aimed to determine the effect of calcium chloride and sodium benzoate on the quality of crude palm oil. The research was done at the Fundamentals of Agricultural Science Laboratory, Faculty of Agriculture, Malikussaleh University, North Aceh Regency. The research was started from September to November 2021. The experimental design used was Factorial Completely Randomized Design. The first factor was Calcium Chloride (C) concentration, 0, 3000, and 4000 ppm. The second factors were Sodium Benzoate (N) concentration, 0, 3000, and 4000 ppm. The results showed that giving a concentration of 3000 ppm sodium benzoate spray was able to reduce the weight loss value of loose fruit and free fatty acids, as well as increase the yield of CPO. There was a very strong relationship between the value of the moisture of the fruit and the level of impurities on the yield produced. For best results it is recommended to use sodium chloride 3000 ppm.
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