An in-vessel filtration system is
a crucial component
in commercial
low-temperature Fischer–Tropsch slurry reactors for the continuous
separation of liquid products and catalysts generated by the reaction.
Periodic back-flushing is key to ensuring the stability and continuity
of the in-vessel filtration system, but it has been relatively unexplored.
In this study, systematically and experimentally, the back-flushing
characteristics of in-vessel filtration are investigated, including
the characteristics of the back-flushing process, the influence of
back-flushing conditions on the recovery of filtration performance,
and some inherent issues for back-flushing. The results indicate that
the in-vessel filtration back-flushing process exhibits four typical
stages: pre-back-flushing stage I, back-flushing stage II, back-flushing
buffering stage III, and reuse stage IV. In stage II, the process
lasts longer due to the incompressibility of the liquid, and it also
has a certain entrainment effect on particles. In stage III, the remaining
liquid level after liquid back-flushing can inhibit the inflow of
liquid, partially preventing a premature decline in filtration performance.
As a result, the recovery of filtration performance following liquid
back-flushing is superior to that of gas. There exists a threshold
value for both gas and liquid back-flushing differential pressures,
beyond which there is no significant improvement in filtration performance.
The recovery of filtration performance varies significantly along
the filter tube height due to differences in flow resistance. During
gas back-flushing, the impact of high-pressure gas on the bed causes
significant pressure fluctuations, affecting the operational stability
of the slurry reactor. Residual particles that cannot be fully removed
by back-flushing exist in the filter tube gaps, and their gradual
accumulation is one of the main causes of filter failure. These findings
contribute to a better understanding of in-vessel filtration back-flushing
and help in the development of improved back-flushing schemes for
industrial plants.