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Background Discoloration affects glass ionomer cement (GIC) color stability due to its brittle nature and microporosity. To counter this, incorporating alternative materials is essential for maintaining color stability. Aim This study aims to determine the color stability and gloss of GIC modified with bioactive chitosan, titanium, zirconia, and hydroxyapatite nanoparticles before and after artificial aging. Materials and methods The study was conducted at Saveetha Research Centre, Saveetha Dental College and Hospitals, Saveetha Institute of Medical and Technical Sciences, Saveetha University, located in Chennai, India. Green-mediated chitosan, titanium, zirconia, and hydroxyapatite (Ch-Ti-Zr-HA) nanoparticles were synthesized using the one-pot synthesis technique. Forty-eight disc-shaped specimens were prepared by incorporating the obtained nanoparticles (nanocomposite) into the GIC, with a diameter of 5 mm and thickness of 2 mm. The specimens were prepared in different concentrations (3%, 5%, and 10%) designated as group I, group II, and group III, respectively. Group IV, serving as the control, consisted of conventional GIC without any modifications. Following preparation, scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) microanalysis confirmed sample elements, and the specimens were submerged in distilled water for a duration of 24 hours prior to the commencement of testing. Subsequently, the specimens underwent artificial aging (thermocycling), between temperatures of 5°C and 55°C, for a total of 30,000 cycles, with a 30-second dwell time. Color change and gloss characteristics were assessed both after 24 hours and following thermocycling using a spectrophotometer and glossometer, respectively. The average color change parameter (ΔE) was measured using Adobe Photoshop. The data obtained were subjected to statistical analysis using an unpaired t-test. Results Significant color stability variations were observed post thermocycling (P = 0.001). Group 2 (5%) exhibited minimal delta E difference (0.508 ± 0.105), indicating superior color stability, while group 4 (control) had maximum difference (1.15 ± 0.187), indicating lower stability. Gloss tests confirmed GIC's polishability, where there were significant differences among all the groups. Conclusion It can be concluded that 5% nanoparticle-modified GIC has better color stability and gloss than conventional GIC. Further studies are needed to analyze the color stability and gloss through dentifrices and other beverages.
Background Discoloration affects glass ionomer cement (GIC) color stability due to its brittle nature and microporosity. To counter this, incorporating alternative materials is essential for maintaining color stability. Aim This study aims to determine the color stability and gloss of GIC modified with bioactive chitosan, titanium, zirconia, and hydroxyapatite nanoparticles before and after artificial aging. Materials and methods The study was conducted at Saveetha Research Centre, Saveetha Dental College and Hospitals, Saveetha Institute of Medical and Technical Sciences, Saveetha University, located in Chennai, India. Green-mediated chitosan, titanium, zirconia, and hydroxyapatite (Ch-Ti-Zr-HA) nanoparticles were synthesized using the one-pot synthesis technique. Forty-eight disc-shaped specimens were prepared by incorporating the obtained nanoparticles (nanocomposite) into the GIC, with a diameter of 5 mm and thickness of 2 mm. The specimens were prepared in different concentrations (3%, 5%, and 10%) designated as group I, group II, and group III, respectively. Group IV, serving as the control, consisted of conventional GIC without any modifications. Following preparation, scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) microanalysis confirmed sample elements, and the specimens were submerged in distilled water for a duration of 24 hours prior to the commencement of testing. Subsequently, the specimens underwent artificial aging (thermocycling), between temperatures of 5°C and 55°C, for a total of 30,000 cycles, with a 30-second dwell time. Color change and gloss characteristics were assessed both after 24 hours and following thermocycling using a spectrophotometer and glossometer, respectively. The average color change parameter (ΔE) was measured using Adobe Photoshop. The data obtained were subjected to statistical analysis using an unpaired t-test. Results Significant color stability variations were observed post thermocycling (P = 0.001). Group 2 (5%) exhibited minimal delta E difference (0.508 ± 0.105), indicating superior color stability, while group 4 (control) had maximum difference (1.15 ± 0.187), indicating lower stability. Gloss tests confirmed GIC's polishability, where there were significant differences among all the groups. Conclusion It can be concluded that 5% nanoparticle-modified GIC has better color stability and gloss than conventional GIC. Further studies are needed to analyze the color stability and gloss through dentifrices and other beverages.
Background and objectiveGlass ionomer cement (GIC), also known as polyalkenoate cement, has been extensively used in dentistry for both luting and restorative purposes. Despite being the first choice for aesthetic restorations due to their chemical bonding ability to teeth, GICs have faced challenges such as low mechanical properties, abrasion resistance, and sensitivity to moisture, leading to the search for improved materials.This study aims to assess the effects of thermocycling on the compressive, flexural strength, and microhardness of green-mediated nanocomposite-modified GIC in comparison to traditional GIC. MethodologyGreen-mediated nanoparticles, consisting of chitosan, titanium, zirconia, and hydroxyapatite (Ch-Ti-Zr-HA), were synthesized using a one-pot synthesis technique to form nanocomposites. These nanocomposites were then incorporated into GIC specimens in varying concentrations (3%, 5%, and 10%), denoted as Group I, Group II, and Group III, respectively. Group IV served as the control, consisting of conventional GIC. To assess the performance of the novel restorative materials over an extended period, compressive strength, flexural strength, and microhardness were measured before and after thermocycling using a universal material testing machine. Furthermore, scanning electron microscopy (SEM) analysis was carried out following the thermocycling process. The collected data were subjected to statistical analysis through oneway analysis of variance (ANOVA) and paired t-tests. ResultsThe findings demonstrated that, in comparison to the control group, both the mean compressive strength and flexural strength, as well as hardness, were notably higher for the 10% and 5% nanocomposite-modified GIC specimens before and after thermocycling (P < 0.05). Notably, there was no notable difference observed between the 5% and 10% concentrations (P > 0.05). These results suggest that incorporating green-mediated nanocomposites (Ch-Ti-Zr-HA) modified GIC at either 5% or 10% concentration levels leads to improved mechanical properties, indicating their potential as promising alternatives in dental restorative materials. ConclusionsBased on our findings, it can be inferred that the 10% and 5% concentrations of green-mediated (Ch-Ti-Zr-HA) modified GIC exhibit superior compressive and flexural strength compared to conventional GIC. Additionally, analysis of the scanning electron microscope (SEM) morphology revealed that green-mediated GIC displays smoother surface characteristics in contrast to conventional GIC. These results underscore the potential advantages of utilizing green-mediated nanocomposite-modified GIC in dental applications, suggesting enhanced mechanical properties and surface quality over conventional.
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