2003
DOI: 10.1081/ppt-120023094
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Annealing Effect on Microhardness and Elastic Constants of PMMA

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Cited by 21 publications
(18 citation statements)
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“…As stated in Ref. [34], the increase in microhardness may be due to the formation of such effects as crosslinking, modifications to chain structure, and modifications to the side group of the polymer. All these reasons may cause C H bonds and methyl groups to be more stable, and rigid structure can be obtained while the duration increases to 3 h. This structural phenomenon was tried to be supported by infrared results explained below.…”
Section: Glass Transition Temperature and Hardness Resultsmentioning
confidence: 98%
“…As stated in Ref. [34], the increase in microhardness may be due to the formation of such effects as crosslinking, modifications to chain structure, and modifications to the side group of the polymer. All these reasons may cause C H bonds and methyl groups to be more stable, and rigid structure can be obtained while the duration increases to 3 h. This structural phenomenon was tried to be supported by infrared results explained below.…”
Section: Glass Transition Temperature and Hardness Resultsmentioning
confidence: 98%
“…Artery surrogates that mimic absorbing and scattering properties of vascular structures with varying compositions were , and imposes an acoustic contrast in our sample [2]. Both tubes first contained air, but we also mimic the presence of blood in the vessels with an infrared absorbing dye (Epolight TM 2057, Epolin, Newark, NJ, USA) dissolved in isopropyl alcohol.…”
Section: Methodsmentioning
confidence: 99%
“…Temperature is a major parameter in the annealing of the polymer. From previous research, the PMMA used for this study has been observed to be most stable if annealed at 80°C below T g [9]. Therefore, annealing was performed at 80°C in order to minimize the residual stress within the structure, and an electricfurnace (Yamato Co., DR200) was used for a uniform heat treatment.…”
Section: Annealing Of the Polymer Microstructurementioning
confidence: 99%
“…An imprinted structure with such residual stress causes rearrangement by the surface tension and stabilized movement of the polymer chain, with its elastic modulus and hardness becoming affected, resulting in the dimensional change of the polymeric optical device. After a certain period of annealing at a given temperature, a polymer structure with residual stress is rearranged and stabilized, and its stress finally becomes relaxed [9]. Therefore, the aim of this study is to fabricate a new polymeric optical device by introducing the imprint technique and evaluating the long-term reliability of the imprinted structure.…”
Section: Introductionmentioning
confidence: 99%