Abstract:The temperature dependent (30 K to 300 K) Doppler broadening of the positron annihilated γ-radiation (DBPAR) measurement has been carried out on single crystalline Bi 2 Sr 2 CaCu 2 O 8+δ (Bi-2212) high T c superconducting sample along two different crystallographic orientations. It has been observed that throughout the temperature range the electron momentum distribution has a relatively large value along the crystallographic c-axis than a-b plane. The temperature dependent DBPARL analysis shows a step like … Show more
“…Use of the two detectors in coincidence [143,144] help to suppress the background in measured Doppler broadened spectrum and hence the contributions of higher momentum electrons (core electrons) can be estimated [145,146]. In the present experiment, the two detector coincidence assembly has been employed here with a HPGe detector (efficiency 13%, energy resolution of 1.3 keV for the 514 keV line of 85 Sr) and a 3 00 Â 3 00 NaI (Tl) crystal coupled to a RCA 8850 photomultiplier tube placed at an angle of 180° [144]. The Doppler broadened electron-positron annihilation c-radiation (CDBEPAR) spectrum has been measured by the HPGe detector.…”
“…The CDBEPAR spectra have been recorded in a dual ADC based -multiparameter data acquisition system (MPA-3 of FAST ComTec., Germany). The CDBEPAR spectra for each sample have been analyzed by evaluating the so-called shape parameter (S-parameter) and wing parameter (W-parameter) [51,134,144]. The S-parameter, calculated as the ratio of counts in the central area of the 511 keV photo peak (|511 keV À E c | 6 0.86 keV) and the total area of the photo peak (|511 keV À E c | 6 4.25 keV), represents the fraction of positrons annihilating with the lower momentum electrons.…”
“…When one attempts to probe the increase/decrease of defects in a sample due to heat treatment or irradiation or substitution etc., usually a high quality sample (sometimes a single crystal of the same material) is taken as reference material [71]. To detect some change, if any, occurs in the defective state of a single-crystalline sample, a temperature-dependent study with reference to the results at room temperature proved to be fruitful [55,144]. To get more 6.…”
Section: Positron Annihilation Spectroscopic Investigation On Zno Sammentioning
“…Use of the two detectors in coincidence [143,144] help to suppress the background in measured Doppler broadened spectrum and hence the contributions of higher momentum electrons (core electrons) can be estimated [145,146]. In the present experiment, the two detector coincidence assembly has been employed here with a HPGe detector (efficiency 13%, energy resolution of 1.3 keV for the 514 keV line of 85 Sr) and a 3 00 Â 3 00 NaI (Tl) crystal coupled to a RCA 8850 photomultiplier tube placed at an angle of 180° [144]. The Doppler broadened electron-positron annihilation c-radiation (CDBEPAR) spectrum has been measured by the HPGe detector.…”
“…The CDBEPAR spectra have been recorded in a dual ADC based -multiparameter data acquisition system (MPA-3 of FAST ComTec., Germany). The CDBEPAR spectra for each sample have been analyzed by evaluating the so-called shape parameter (S-parameter) and wing parameter (W-parameter) [51,134,144]. The S-parameter, calculated as the ratio of counts in the central area of the 511 keV photo peak (|511 keV À E c | 6 0.86 keV) and the total area of the photo peak (|511 keV À E c | 6 4.25 keV), represents the fraction of positrons annihilating with the lower momentum electrons.…”
“…When one attempts to probe the increase/decrease of defects in a sample due to heat treatment or irradiation or substitution etc., usually a high quality sample (sometimes a single crystal of the same material) is taken as reference material [71]. To detect some change, if any, occurs in the defective state of a single-crystalline sample, a temperature-dependent study with reference to the results at room temperature proved to be fruitful [55,144]. To get more 6.…”
Section: Positron Annihilation Spectroscopic Investigation On Zno Sammentioning
“…The CDBEPARL spectrum has been analyzed by evaluating the ratio curve analysis19,20 . In each CDBEPARL spectrum the S-parameter19 is calculated as the ratio of the counts in the central area of the 511 keV photo peak (| 511 keV -E γ | ≤ 0.85 keV) and the total areaof the photo peak (| 511 keV -E γ | ≤ 4.25 keV). Defects in SnO 2 were created by using 96 MeV 16 O 8+ ions from 15 UD pelletron at IUAC, New-Delhi.…”
mentioning
confidence: 99%
“…It is worth mentioning that PAS spectroscopy is very much sensitive to vacancy type open volume defects in solid materials 2,6,19. .…”
Room temperature ferromagnetic ordering has been observed in high purity polycrystalline SnO 2 sample due to irradiation of 96 MeV oxygen ions. Ab initio calculation in the density functional theory indicates that tin vacancies are mainly responsible for inducing magnetic moment in SnO 2 whereas oxygen vacancies in SnO 2 do not contribute any magnetic moment. Positron annihilation spectroscopy has been employed to characterize the chemical identity of irradiation generated defects in SnO 2 .Results indicate the dominant presence of Sn vacancies in O ion irradiated SnO 2 . The irradiated sample turns out to be ferromagnetic at room temperature.
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