Analytic approximation for incoherent scattered X-ray intensities

Hajdu, F.

doi:10.1107/s0567739471000159

Cited by 85 publications

(29 citation statements)

References 5 publications

(5 reference statements)

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“…Air scattering and sample environment background (kapton tape plus millipore support) were independently measured, corrected for the sample transmittivity, then subtracted. The Compton scattering background was evaluated using the calculated values reported in the references (Hajdu, 1971;Palinkas, 1973). The diffractograms recorded near the Zr K edge contain the K¯uorescence contribution, I K , that cannot be resolved from the elastic signal by the detector resolution.…”

Section: Xrs and Das Data Analysis And Resultsmentioning

confidence: 99%

Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO₂–ZrO₂system

Meneghini¹,

Gualtieri²,

Siligardi³

1999

J Appl Crystallogr

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The structure of a CaO±SiO 2 ±ZrO 2 -based glass ceramic has been investigated by X-ray diffraction, X-ray absorption spectroscopy and differential anomalous scattering techniques as a function of the thermal treatment of the sample. The microstructure of the glass has been investigated at room temperature, before the recrystallization of the glass ceramic, and on two samples annealed at 1073 and 1273 K for 1 h to follow the early stages of nucleation of the quartz and wollastonite crystalline phases. Indications on the roles of Ca, Si and Zr during the devitri®cation process are given.

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Section: Xrs and Das Data Analysis And Resultsmentioning

confidence: 99%

Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO₂–ZrO₂system

Meneghini¹,

Gualtieri²,

Siligardi³

1999

J Appl Crystallogr

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“…The scattered X-ray intensities so obtained at ambient temperature were corrected for background, polarization, absorption, and Compton scattering, and normalized to the coherent scattering intensity of the stoichiometric unit, in accordance with the usual procedure [23]. Atomic scattering factors and Compton scattering factors were taken from the literature [24,25]. Thus, the experimental structure factors and radial distribution functions were obtained.…”

Section: X-ray Diffractionmentioning

confidence: 99%

The Local Structure of Liquid TiCl4 Analyzed by X-Ray Diffraction and Raman Spectroscopy

Iwadate

Ohkubo

2013

Zeitschrift Für Naturforschung A

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Structural analyses were performed to determine the local structure of liquid TiCl 4 using laboratory-scale X-ray diffraction and Raman spectroscopy from which the existence of tetrahedral TiCl 4 molecules in the liquid was definitely confirmed. Conventionally, in molten salts, the valence increase of the central metal ion, for example in the range from 1 to 3, leads to more complicated liquid structures, yet a further increase in valence is usually accompanied by an enhanced covalency, forming stable tetrahedral molecules like e. g. CCl 4 . We discuss the intermolecular structure of TiCl 4 liquid as well as the intramolecular one.

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“…Tabulated values of the atomic scattering factor (Cromer & Waber, 1965) and incoherent scattering factors (Hajdu, 1971) were used for obtaining the independent scattering curves. The corrected intensities Icorr were scaled to electron units (Ie.u.)…”

Section: Recording Of Intensities and Calculation Of The Radial Distrmentioning

confidence: 99%

X-ray diffraction studies on the arrangement of atoms in carbon blacks. I. Results of radial distribution analysis

Sanyal¹,

Samantaray²,

Mitra³

1982

Acta Cryst Sect A

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Analytic approximation for incoherent scattered X-ray intensities

Cited by 85 publications

References 5 publications

Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO₂–ZrO₂system

Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO₂–ZrO₂system

The Local Structure of Liquid TiCl4 Analyzed by X-Ray Diffraction and Raman Spectroscopy

X-ray diffraction studies on the arrangement of atoms in carbon blacks. I. Results of radial distribution analysis

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Analytic approximation for incoherent scattered X-ray intensities

Cited by 85 publications

References 5 publications

Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO2–ZrO2system

Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO2–ZrO2system

The Local Structure of Liquid TiCl4 Analyzed by X-Ray Diffraction and Raman Spectroscopy

X-ray diffraction studies on the arrangement of atoms in carbon blacks. I. Results of radial distribution analysis

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Product

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Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO₂–ZrO₂system

Differential anomalous wide-angle X-ray scattering and X-ray absorption experiments to investigate the formation of glass ceramics in the CaO–SiO₂–ZrO₂system