Analysis of zone-melted ultra-pure organic compoundsA new quantitative differential thermal analysis method

Thermal analysis

“…Friedenberg and Jannke (143) extended Herrington's (180) work, developing and applying expressions relating the difference in AT slopes obtained on heating and cooling milligram samples and Cu cone reference in a Dewar. Although the experimental procedure was long, heating rate of 0.016°C /minute with a 5-hour soak time, the establishment of method constants would make routine measurements rapid and automatic with a specific system.…”