Analysis of vapor phase butane nitration products by gas chromatography

Fear, Dennis Lee; Burnet, G.

doi:10.1016/s0021-9673(01)99422-1

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1967

1978

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Cited by 7 publications

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“…Early analytical problems are also described in the review paper by Albright (1966). Gas chromatographic methods are now used which give accurate and complete product analyses (Fear and Burnet, 1965). An important part of the work now being reported deals with development of an on-line chromatographic technique which eliminates the need to collect, cool, and separate the reactor products prior to analysis (Johnnie et al, 1968).…”

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Process Design Data for the Vapor-Phase Nitration of Butane

Hankinson¹,

Burnet²

1971

Ind. Eng. Chem. Proc. Des. Dev.

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A modified molten salt reactor and an on-line gas chromatographic analysis system were used to obtain yield, conversion, and product distribution data for the vaporphase nitration of normal butane. The effects of temperature (385°t o 455°C ), mole ratio of hydrocarbon to nitric acid (3-to-7) and total reactant flow rate (0.433 to 1.235 g-mol/min) were studied. Statistical methods were applied to correlate and

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